|
TT
|
CHỈ TIÊU
|
PHƯƠNG PHÁP THỬ NGHIỆM
|
LOD
|
|
IV. DƯ LƯỢNG NITRIT VÀ NITRAT
|
|
20.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7806:2007
|
1 mg/Kg
|
|
21.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7806:2007
|
1 mg/Kg
|
|
V. KIM LOẠI NẶNG VÀ CÁC KIM LOẠI KHÁC
|
|
22.
|
Arsen (As)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
23.
|
Thủy ngân (Hg) (**)
|
AOAC 974.14 (2011) & TCVN 7993:2009
|
0.01 mg/Kg
|
|
24.
|
Cadimi (Cd)
|
AOAC 999.11 (2011)
|
0.005 mg/Kg
|
|
25.
|
Chì (Pb)
|
AOAC 999.11 (2011)
|
0.01 mg/Kg
|
|
26.
|
Đồng (Cu)
|
AOAC 999.11 (2011)
|
0.2 mg/Kg
|
|
27.
|
Canxi (Ca)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
28.
|
Selen (Se)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
29.
|
Kali (K)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
30.
|
Magie (Mg)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
31.
|
Mangan (Mn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
32.
|
Sắt (Fe)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
33.
|
Natri (Na)
|
AOAC 999.23
|
0.5 mg/Kg
|
|
34.
|
Antimo (Sb)
|
TK.AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
35.
|
Kẽm (Zn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
VI. CÁC THÀNH PHẦN KHÁC
|
|
36.
|
Acid amine (gồm 20 acid amine)(**)
|
TK.EZ : faast (LCMSMS)
|
10.0 mg/kg
|
|
|
Glycine(**)
|
10.0 mg/kg
|
|
|
Alanine(**)
|
|
|
|
Serine(**)
|
|
|
|
Proline(**)
|
|
|
|
Valine(**)
|
|
|
|
Threonine(**)
|
|
|
|
Methionine(**)
|
|
|
|
Trans-4-hydroxy-proline(**)
|
|
|
|
Arginine(**)
|
|
|
|
Aspartic acid(**)
|
|
|
|
Glutamic acid(**)
|
|
|
|
Cysteine(**)
|
|
|
|
Lysine(**)
|
|
|
|
Histidine(**)
|
|
|
|
Tyrosine(**)
|
|
|
|
Cystine(**)
|
|
|
|
Leucine _ Isoleucine(**)
|
|
|
|
Phenylalamine(**)
|
|
|
|
Saturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
38.
|
Monounsaturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
39.
|
Polyunsaturated fatty acid(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
40.
|
Trans fat(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
41.
|
Omega 3(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
42.
|
Omega 6(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
43.
|
Omega 9(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
44.
|
DHA(**)
|
TK.AOAC 996.06 for food (GC/FID)
|
20mg/kg
|
|
45.
|
Cholesterol(**)
|
TK.AOAC 970.51 (LCMSMS)
|
1.0mg/kg
|
|
46.
|
DEHP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/kg
|
|
47.
|
DINP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/kg
|
|
VII. DƯ LƯỢNG THUỐC KHÁNG SINH
|
|
48.
|
Họ Tetracyline
|
TK. AOAC 995.09 (LCMSMS)
|
|
|
|
Tetracyclin
|
100.0mg/kg
|
|
|
Chlortetracyclin
|
100.0mg/kg
|
|
|
Oxytetracyclin
|
100.0mg/kg
|
|
49.
|
Họ Sulfonamide
|
TK. Journal of Chro A 1177 (LCMSMS)
|
|
|
|
Sulfamethoxazole
|
20.0mg/kg
|
|
|
Sulfadicine
|
20.0mg/kg
|
|
|
Sulfadiazine
|
20.0mg/kg
|
|
|
Sulfathiazole
|
20.0mg/kg
|
|
|
Sulfamidine
|
20.0mg/kg
|
|
50.
|
Beta-Lactamine(**)
|
TK.Analytical Chimica Acta 520 ( 2004), p14-32, 590 – 3722 EN, Agilent (LCMSMS)
|
|
|
|
Amipicillin(**)
|
1.0mg/kg
|
|
|
Amoxycillin(**)
|
1.0mg/kg
|
|
|
Benzylpenicillin(**)
|
1.0mg/kg
|
|
51.
|
Streptomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
100mg/kg
|
|
52.
|
Spiramycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
53.
|
Gentamycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
54.
|
Tylosin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
10.0mg/kg
|
|
55.
|
Lincomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
10.0mg/kg
|
|
56.
|
Họ Nitroimidazole(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
|
|
|
Ronidazole(**)
|
1.0mg/kg
|
|
|
Omidazole(**)
|
1.0mg/kg
|
|
|
Metronidazole(**)
|
1.0mg/kg
|
|
|
Ipronidazole(**)
|
1.0mg/kg
|
|
|
Dimetridazole(**)
|
1.0mg/kg
|
|
|
Tinidazole(**)
|
50.0mg/kg
|
|
VIII. VITAMIN
|
|
57.
|
Vitamin A(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
58.
|
Vitamin D3(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
59.
|
Vitamin K
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
60.
|
Vitamin E(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
61.
|
Vitamin C
|
Ref Journal of Chromatography A
UHPLC-DAD
|
1.0mg/kg
|
|
62.
|
Vitamin B1
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
63.
|
Vitamin B2
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
64.
|
Vitamin B3 (Nicotinamide)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
65.
|
Vitamin B5 (Acid pantothenic)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
66.
|
Vitamin B6
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
67.
|
Vitamin B9 (Folic acid)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
68.
|
Vitamin B12
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
69.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/kg
|
|
IX. ĐỊNH LƯỢNG DƯ LƯỢNG THUỐC BẢO VỆ THỰC VẬT
|
|
70.
|
Dư lượng thuốc bảo vệ thực vật gốc Carbamat
|
TK.AOAC 2007.01 (LCMSMS)
|
|
|
|
Isoprocarb
|
0.01mg/kg
|
|
|
Aldicarb sulfone
|
0.01mg/kg
|
|
|
Aldicarb (*)
|
0.005mg/kg
|
|
|
Aldicarb sulfoxide (*0
|
0.005mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran (*)
|
0.02mg/kg
|
|
|
Carbaryl (*)
|
0.02mg/kg
|
|
|
Methomyl (*)
|
0.01mg/kg
|
|
|
Oxamyl (*)
|
0.01mg/kg
|
|
|
Thiodicarb
|
0.01mg/kg
|
|
|
Methiocarb (*)
|
0.005mg/kg
|
|
|
Fenobucarb
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran-3-Hydroxy
|
0.01mg/kg
|
|
71.
|
Dư lượng thuốc bảo vệ thực vật gốc Clo
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
2,4'-DDD
|
0.01mg/kg
|
|
|
4,4'-DDD
|
0.01mg/kg
|
|
|
2,4'-DDE
|
0.01mg/kg
|
|
|
4,4'-DDE
|
0.01mg/kg
|
|
|
2,4'-DDT
|
0.01mg/kg
|
|
|
4,4'-DDT
|
0.01mg/kg
|
|
|
Alpha-Lindan
|
0.005mg/kg
|
|
|
Gamma-Lindan
|
0.005mg/kg
|
|
|
Beta-Lindan
|
0.005mg/kg
|
|
|
Isodrin
|
0.003mg/kg
|
|
|
Aldrin
|
0.003mg/kg
|
|
|
Dieldrin
|
0.003mg/kg
|
|
|
Endrin
|
0.003mg/kg
|
|
|
Hexachloro-Benzene
|
0.003mg/kg
|
|
|
Heptachlor
|
0.003mg/kg
|
|
|
Heptachlor epoxide
|
0.003mg/kg
|
|
|
Endosulfan I
|
0.01mg/kg
|
|
|
Endosulfan II
|
0.01mg/kg
|
|
72.
|
Dư lượng thuốc bảo vệ thực vật gốc Phosphor
|
TK.AOAC 2007.01 (LCMSMS)
|
-
|
|
|
Diazinon
|
0.01mg/kg
|
|
|
Parathion Methyl
|
0.01mg/kg
|
|
|
Malathion
|
0.01mg/kg
|
|
|
Chlorpyrifos
|
0.01mg/kg
|
|
|
Parathion ethyl
|
0.01mg/kg
|
|
|
Bromophos methyl
|
0.01mg/kg
|
|
|
Bromophos ethyl
|
0.01mg/kg
|
|
|
Ethion
|
0.01mg/kg
|
|
73.
|
Dư lượng thuốc bảo vệ thực vật gốc Cúc
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
Cypermethrin
|
0.025mg/kg
|
|
|
Deltamethrin
|
0.025mg/kg
|
|
|
Permethrin
|
0.05mg/kg
|
|
|
Fenvalerate
|
0.05mg/kg
|
|
|
Resmethrine
|
0.05mg/kg
|
|
|
Fenthropathrine
|
0.05mg/kg
|
|
74.
|
Abamectine(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
75.
|
Acephate (**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
76.
|
Carbendazim (**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
77.
|
Chlorantraniliprole(**)
|
AOAC 2007.01 (LCMSMS)
|
0.1mg/kg
|
|
78.
|
Difenoconazole (**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
79.
|
Emamectine benzoate(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
80.
|
Flusilazole(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
81.
|
Imidacloprid (**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
82.
|
Indoxacarb(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
83.
|
Paraquat(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
84.
|
Pirimicarb (**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
85.
|
Propiconazole(**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
86.
|
Tebuconazole(**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
87.
|
Thiamethoxam(**)
|
AOAC 2007.01 (LCMSMS)
|
0.01mg/kg
|
|
88.
|
2,4D(**)
|
AOAC 2007.01 (LCMSMS)
|
0.005mg/kg
|
|
89.
|
Triclorfon(**)
|
AOAC 2007.01 (GCMS)
|
0.05mg/kg
|
|
90.
|
Cyfluthrin(**)
|
AOAC 2007.01 (GCMS)
|
0.05mg/kg
|
|
91.
|
Propagite(**)
|
AOAC 2007.01 (GCMS)
|
0.05mg/kg
|
|
X. PHỤ GIA THỰC PHẨM
|
|
92.
|
Acid citric (E330)
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
20.0mg/kg
|
|
93.
|
Acid Tartaric (E334)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
94.
|
Acid malic (E296)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
95.
|
Acid fumaric (E297)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
96.
|
Acid lactic (E270)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
97.
|
Acid ascorbic / Natri ascorbate
|
Ref Journal of Chromatography A
UHPLC-DAD
|
1.0mg/kg
|
|
98.
|
Alpha-Tocopherol(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/kg
|
|
99.
|
BHA (Butylated hydroxyanisol)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
100.
|
BHT (Butylated hydroxytoluene)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
101.
|
TBHQ (Tert-Butyl hydroquinone)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
102.
|
Aicd propionic(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
103.
|
Benzoyl peroxyd(**)
|
(HPLC/UV)
|
10.0mg/kg
|
|
104.
|
Aspartame (E951)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10.0mg/kg
|
|
105.
|
Acesulfam K (E950)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
10.0mg/kg
|
|
106.
|
Saccharine (E954)(**)
|
TK. TCVN 8471 : 2010 (HPLC/UV)
|
0.5mg/kg
|
|
107.
|
Maltitol(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
108.
|
Mannitol(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
109.
|
Sorbitol(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
110.
|
Inositol(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.01%
|
|
111.
|
Isomalt(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
112.
|
Isomaltulose(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
113.
|
Sucralose(**)
|
TK. HPLC – High Performance Liquid Chromatoghapht
|
0.50%
|
|
114.
|
Glucose(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
115.
|
Fructose(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
116.
|
Lactose(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
117.
|
Saccharose(**)
|
TK. GC - Chrompack application note, Varian application 708
|
0.50%
|
|
118.
|
Monosodium Glutamate(**)
|
TK. EZ : faast (LCMSMS)
|
10.0mg/kg
|
|
XI. THUỐC TĂNG TRƯỞNG _ HORMON
|
|
119.
|
Bea agonist
|
LC/MS/MS
|
|
|
|
Salbutamol
|
LC/MS/MS
|
0.3mg/kg
|
|
|
Clenbuterol
|
LC/MS/MS
|
0.3mg/kg
|
|
|
Ractopamine
|
LC/MS/MS
|
0.3mg/kg
|
|
120.
|
Dexamethasone(**)
|
TK. Journal of chromatoghaphy B, volume 862, issue 1-2, p119 -124
|
0.30µg/kg
|
|
121.
|
Hormons(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
|
|
|
Progesterol(**)
|
50µg/kg
|
|
|
Estradiol(**)
|
50µg/kg
|
|
|
Testosterone(**)
|
50µg/kg
|
|
|
Dietylstylbestrole(**)
|
50µg/kg
|
|
XII. ĐỘC TỐ NẤM MỐC
|
|
122.
|
Aflatoxin Tổng(**)
|
TK.AOAC 991.31 (LC/MS/MS)
|
1.0µg/kg
|
|
123.
|
Aflatoxin/chất (B1, B2, G1, G2)(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/kg
|
|
124.
|
Ochratoxin A(**)
|
TK. AOAC 2000.09(LC/MS/MS)
|
1.0µg/kg
|
|
125.
|
Melamine(**)
|
TK. FDA 4396 (LC/MS/MS)
|
50µg/kg
|
|
126.
|
Deoxynivalenol (DON)(**)
|
TK.AOAC 986.18 (LC/MS/MS)
|
50µg/kg
|
|
127.
|
Zearalenone(**)
|
TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)
|
1.0µg/kg
|
|
128.
|
Aflatoxin M1(**)
|
AOAC 986.16:2002 (HPLC-UV)
|
0.01µg/kg
|
|
XIII. VI SINH
|
|
129.
|
Tổng số vi khuẩn hiếu khí
|
TCVN 4884:2005 (ISO 4833:2003)
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
130.
|
Coliforms
|
TCVN 6848:2007 ISO 4832:2007
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
131.
|
E. coli
|
TCVN 7924-2:2008 ISO 16649-2:2001
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
132.
|
Clostridium perfringens
|
TCVN 4991 : 2005, ISO 7937 : 2004
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
133.
|
Bacillus cereus
|
TCVN 4992:2005, ISO 7932:1987
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
134.
|
Staphylococcus aureus
|
TCVN 4830-1 : 2005, ISO 6888-1 : 1999
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
135.
|
Tổng nấm men - nấm mốc
|
TCVN 8275-1:2010, ISO 21527-1:2008
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
136.
|
Salmonella
|
TCVN 4829:2005, ISO 6579:2002
|
_
|
|
137.
|
Enterobacteriaceae
|
TCVN 5518-2:2007, ISO 21528-2:2004
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
138.
|
Phương pháp định lượng vi khuẩn
acid lactic ưa nhiệt trung bình
-Kỹ thuật đếm khuẩn lạc ở 300C (*)
|
TCVN7906-1:2008
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
139.
|
Định lượngLactobacillus acidophilus
giả định trên môi trường chọn lọc
- kỹ thuật đếm khuẩn lạc ở 370C (*)
|
TCVN 7849:2008(ISO 20128:2006)
|
Dạng lỏng: 1 CFU/mL, Dạng khác: 10 CFU/g
|
|
140.
|
Listeria monocytogenes
|
TCVN 7700-1:2007 (ISO 11290-1:1996 sửa đổi 1:2004)
|
10 CFU/g
|