|
TT
|
CHỈ TIÊU
|
PHƯƠNG PHÁP THỬ NGHIỆM
|
GIỚI HẠN/ĐƠN VỊ
|
|
III. VITAMIN
|
|
15.
|
Vitamin A(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
16.
|
Vitamin D3(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
17.
|
Vitamin E(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
18.
|
Vitamin C
|
Ref Journal of Chromatography A
UHPLC-DAD
|
1.0mg/kg
|
|
19.
|
Vitamin B1
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
20.
|
Vitamin B2
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
21.
|
Vitamin B3 (Nicotinamide)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
22.
|
Vitamin B5 (Acid pantothenic)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
23.
|
Vitamin B6
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
24.
|
Vitamin B9 (Floic acid)
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
25.
|
Vitamin B12
|
Ref Journal of Chromatography A
UHPLC-DAD
|
0.1mg/kg
|
|
26.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/kg
|
|
IV. DƯ LƯỢNG NITRIT VÀ NITRAT
|
|
27.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7767:2007
|
1 mg/Kg
|
|
28.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7767:2007
|
1 mg/Kg
|
|
V. KIM LOẠI NẶNG VÀ CÁC KIM LOẠI KHÁC
|
|
29.
|
Arsen (As)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
30.
|
Thủy ngân (Hg)(**)
|
AOAC 974.14 (2011)
|
0.01 mg/Kg
|
|
31.
|
Cadimi (Cd)
|
AOAC 999.11 (2011)
|
0.005 mg/Kg
|
|
32.
|
Chì (Pb)
|
AOAC 999.11 (2011)
|
0.01 mg/Kg
|
|
33.
|
Đồng (Cu)
|
AOAC 999.11 (2011)
|
0.2 mg/Kg
|
|
34.
|
Canxi (Ca)
|
AOAC 999.23
|
|
|
35.
|
Selen (Se)
|
AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
36.
|
Kali (K)
|
AOAC 999.23
|
|
|
37.
|
Magie (Mg)
|
AOAC 999.23
|
|
|
38.
|
Mangan (Mn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
39.
|
Sắt (Fe)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
40.
|
Natri (Na)
|
AOAC 999.23
|
|
|
41.
|
Antimo (Sb)
|
TK.AOAC 986.15 (2011)
|
0.01 mg/Kg
|
|
42.
|
Kẽm (Zn)
|
AOAC 999.11 (2011)
|
0.5 mg/Kg
|
|
VI. CÁC THÀNH PHẦN KHÁC
|
|
43.
|
Acid amine (gồm 20 acid amine)(**)
|
TK.EZ : faast (LCMSMS)
|
10.0 mg/kg
|
|
|
Glycine(**)
|
10.0 mg/kg
|
|
|
Alanine(**)
|
|
|
|
Serine(**)
|
|
|
|
Proline(**)
|
|
|
|
Valine(**)
|
|
|
|
Threonine(**)
|
|
|
|
Methionine(**)
|
|
|
|
Trans-4-hydroxy-proline(**)
|
|
|
|
Arginine(**)
|
|
|
|
Aspartic acid(**)
|
|
|
|
Glutamic acid(**)
|
|
|
|
Cysteine(**)
|
|
|
|
Lysine(**)
|
|
|
|
Histidine(**)
|
|
|
|
Tyrosine(**)
|
|
|
|
Cystine(**)
|
|
|
|
Leucine _ Isoleucine(**)
|
|
|
|
Phenylalamine(**)
|
|
|
|
Saturated fatty acid(**)
|
TK.AOAC 996.06 for food,TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
45.
|
Monounsaturated fatty acid(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
46.
|
Polyunsaturated fatty acid(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
47.
|
Trans fat(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
48.
|
Omega 3(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
49.
|
Omega 6(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
50.
|
Omega 9(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
51.
|
DHA(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
52.
|
Cholesterol(**)
|
TK.AOAC 970.51 (LCMSMS)
|
1.0mg/kg
|
|
53.
|
DEHP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/l
|
|
54.
|
DINP(**)
|
TK. AOAC 2000.01 (GCMS)
|
0.1mg/l
|
|
55.
|
Melamine(**)
|
TK. FDA 4396 (LC/MS/MS)
|
50µg/kg
|
|
VII. PHỤ GIA
|
|
56.
|
Monosodium Glutamate(**)
|
TK. EZ : faast (LCMSMS)
|
10.0mg/kg
|
|
57.
|
Disodium Isosinate(**)
|
TK : HPLC Application Note 820435 (HPLC/UV)
|
5.0mg/kg
|
|
58.
|
Disodium Guanylate(**)
|
TK : HPLC Application Note 820435 (HPLC/UV)
|
5.0mg/kg
|
|
59.
|
Natri benzoate / Acid benzoic
|
Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD
|
10.0mg/l
|
|
60.
|
Kali sorabte/ Acid sorbic
|
Ref Journal of Chromatography A
UHPLC-DAD
|
10.0mg/l
|
|
61.
|
Aicd propionic(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
62.
|
Aicd fomic(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
63.
|
Acid acetic / Natri acetate(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/l
|
|
64.
|
Benzoyl peroxyd(**)
|
(HPLC/UV)
|
10.0mg/kg
|
|
65.
|
Paraben(**)
|
TK. AOAC 983.16 (HPLC/UV)
|
|
|
66.
|
Butylparaben (Butyl-4-hydroxybenzoate)(**)
|
TK. AOAC 983.16 (HPLC/UV)
|
10.0mg/kg
|
|
|
Ethylparaben (Ethyl-4-hydroxybenzoate)(**)
|
10.0mg/kg
|
|
|
Methylparaben (Methyl-4-hydroxybenzoate)(**)
|
10.0mg/kg
|
|
|
Propylparaben (Propyl-4-hydroxybenzoate)(**)
|
10.0mg/kg
|
|
|
Heptylparaben (Heptyl-4-hydroxybenzoate)(**)
|
10.0mg/kg
|
|
67.
|
Acid citric (E330)
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
20.0mg/kg
|
|
68.
|
Acid Tartaric (E334)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
69.
|
Acid malic (E296)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
70.
|
Acid fumaric (E297)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
71.
|
Acid lactic (E270)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
72.
|
Acid ascorbic / Natri ascorbate
|
Ref Journal of Chromatography A
UHPLC-DAD
|
1.0mg/kg
|
|
73.
|
Alpha-Tocopherol(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/kg
|
|
74.
|
BHA (Butylated hydroxyanisol)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
75.
|
BHT (Butylated hydroxytoluene)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
76.
|
TBHQ (Tert-Butyl hydroquinone)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
77.
|
Beta-caroten(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/l
|
|
78.
|
Curcumin(**)
|
(HPLC/UV)
|
10.0mg/kg
|
|
79.
|
Orange II(**)
|
TK : LGC/GC/2007/005,Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
0.1mg/kg
|
|
80.
|
Parared(**)
|
TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
0.1mg/kg
|
|
81.
|
Ponceau 4R(**)
|
TK : LGC/GC/2007/005 Analysis of illegal Dyes in chilli Powder by LC-UV (HPLC/UV
|
10.0mg/kg
|
|
82.
|
Rhodamine B(**)
|
TK : Method No PV 2072, OSHA, USD (HPLC/UV)
|
0.1mg/kg
|
|
83.
|
Riboflavin(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/kg
|
|
84.
|
Sudan(**)
|
TK : AOAC International Workshop " Food to Dyes For" (HPLC/UV)
|
0.1mg/kg
|
|
85.
|
Sudan I(**)
|
0.1mg/kg
|
|
|
Sudan II(**)
|
0.1mg/kg
|
|
|
Sudan III(**)
|
0.1mg/kg
|
|
|
Sudan IV(**)
|
0.1mg/kg
|
|
86.
|
Sunset yellow(**)
|
TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)
|
10.0mg/kg
|
|
87.
|
Tartazine(**)
|
TK : JFDA Vol 14, No3, 2006, P284 – 291 (HPLC/UV)
|
10.0mg/kg
|
|
VIII. DƯ LƯỢNG THUỐC BẢO VỆ THỰC VẬT
|
|
88.
|
Thuốc bảo vệ thực vật gốc Carbamat
|
TK.AOAC 2007.01 (LCMSMS)
|
|
|
|
Isoprocarb
|
0.01mg/kg
|
|
|
Aldicarb sulfone
|
0.01mg/kg
|
|
|
Aldicarb
|
0.01mg/kg
|
|
|
Aldicarb sulfoxide
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran
|
0.01mg/kg
|
|
|
Carbaryl
|
0.01mg/kg
|
|
|
Methomyl
|
0.01mg/kg
|
|
|
Oxamyl
|
0.01mg/kg
|
|
|
Thiodicarb
|
0.01mg/kg
|
|
|
Methiocarb
|
0.01mg/kg
|
|
|
Fenobucarb
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran-3-Hydroxy
|
0.01mg/kg
|
|
89.
|
Thuốc bảo vệ thực vật gốc Clo
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
2,4'-DDD
|
0.05mg/kg
|
|
|
4,4'-DDE
|
0.05mg/kg
|
|
|
2,4'-DDE
|
0.05mg/kg
|
|
|
Alpha-Lindan
|
0.05mg/kg
|
|
|
Gamma-Lindan
|
0.05mg/kg
|
|
|
Beta-Lindan
|
0.05mg/kg
|
|
|
Isodrin
|
0.05mg/kg
|
|
|
Aldrin
|
0.05mg/kg
|
|
|
Dieldrin
|
0.05mg/kg
|
|
|
Hexachloro-Benzene
|
0.05mg/kg
|
|
|
Heptachlor
|
0.05mg/kg
|
|
|
Heptachlor epoxide
|
0.05mg/kg
|
|
|
Endosulfan I
|
0.05mg/kg
|
|
90.
|
Thuốc bảo vệ thực vật gốc Phosphor
|
TK.AOAC 2007.01 (GCMS)
|
0.05mg/kg
|
|
|
Fenthion
|
0.05mg/kg
|
|
|
Diazinon
|
0.05mg/kg
|
|
|
Parathion Methyl
|
0.05mg/kg
|
|
|
Malathion
|
0.05mg/kg
|
|
|
Chlorpyrifos
|
0.05mg/kg
|
|
|
Parathion ethyl
|
0.05mg/kg
|
|
|
Bromophos methyl
|
0.05mg/kg
|
|
|
Bromophos ethyl
|
0.05mg/kg
|
|
|
Ethion
|
0.05mg/kg
|
|
91.
|
Thuốc bảo vệ thực vật gốc Cúc
|
TK.AOAC 2007.01 (GCMS)
|
0.05mg/kg
|
|
|
Cypermethrin
|
0.05mg/kg
|
|
|
Deltamethrin
|
0.05mg/kg
|
|
|
Permethrin
|
0.05mg/kg
|
|
|
Fenvalerate
|
0.05mg/kg
|
|
|
Resmethrine
|
0.05mg/kg
|
|
|
Fenthropathrine
|
0.05mg/kg
|
|
IX. ĐỘC TỐ NẤM MÓC
|
|
92.
|
Aflatoxin Tổng(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/kg
|
|
93.
|
Aflatoxin/chất (B1, B2, G1, G2)(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/kg
|
|
94.
|
Ochratoxin A(**)
|
AOAC 2000.09(LC/MS/MS)
|
1.0µg/kg
|
|
95.
|
Deoxynivalenol (DON)(**)
|
TK.AOAC 986.18 (LC/MS/MS)
|
50µg/kg
|
|
96.
|
Zearalenone(**)
|
TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)
|
1.0µg/kg
|
|
X. VI SINH
|
|
97.
|
Tổng số vi khuẩn hiếu khí (*)
|
TCVN 4884:2005, ISO 4833:2003
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
98.
|
Coliforms(*)(CFU)
|
TCVN 6848:2006, ISO 4832:2007
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
99.
|
Coliforms(*)(CFU)
|
AOAC 991.14:2011 (Petrifilm)
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
100.
|
E.coli(*) (CFU)
|
AOAC 991.14:2011( Petrifilm)
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
101.
|
E.coli(*) (CFU)
|
TCVN 7924-2:2008, ISO 16649-2:2001
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
102.
|
Staphylococcus aureus (*)
|
TCVN 4830-1:2005, (ISO 6888-1:2003)
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
103.
|
Staphylococcus aureus(*)
|
AOAC 2003.07:2011 (Petrifilm)
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
104.
|
Clostridium perfringens(*)
|
TCVN 4991:2005 (ISO 7937:2004)
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
105.
|
Bacillus cereus(*)
|
TCVN 4992:2005, ISO 7932:2004
|
Dạng lỏng:1 CFU/mL, Dạng khác:10 CFU/g
|
|
106.
|
Nấm men-Nấm mốc(*)
|
TCVN 8275-2:2010, ISO 21527-2:2008 (dạng rắn)
|
10 CFU/g
|